反应详情

温度

67.5 °C

A mixture of methyl 3-(4-chlorophenyl)-2,2dimethoxypropionate (6.09 g) and formic acid (27 ml) was heated at 65 to 70° C. for 4 hours with stirring. The reaction mixture was cooled and extracted with methylene chloride. The extract was washed with water, dried over magnesium sulfate and evaporated in vacuo to give methyl 3-(4-chlorophenyl)propionate.

1. temperatureThe reaction mixture was cooled
2. extractionextracted with methylene chloride
3. washThe extract was washed with water
4. dry with materialdried over magnesium sulfate
5. customevaporated in vacuo