HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ac-Orn(Boc)-Pro-Gly-OBzl → Ac-Orn-Pro-Gly-OBzl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ac-Orn(Boc)-Pro-Gly-OBzl | HCID 131715813 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | Ac-Orn-Pro-Gly-OBzl | HCID 13853221 | — |
Reaction Steps
2.0 g of Ac-Orn(Boc)-Pro-Gly-OBzl are dissolved in 5 ml of trifluoroacetic acid, and the solution is stirred at room temperature for 1 hour. After evaporation under high vacuum, 2.1 g of the trifluoroacetate of Ac-Orn-Pro-Gly-OBzl remain. Rf (system 2)=0.3; MS (FAB): 419 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04797471 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-6a0a3c5464324f02a704a55840cb2a6b |
| Source note | uspto-grants-1989_01 |