HRID2291651

反应详情

EQUATION

反应方程式

REACTANTS

反应物

反应SMILES：CC(=O)N[C@@H](CCCNC(=O)OC(C)(C)C)C(=O)N1CCC[C@H]1C(=O)NCC(=O)OCc1ccccc1

HCID131715813

未命名化合物

PRODUCTS

产物

反应SMILES：CC(=O)N[C@@H](CCCN)C(=O)N1CCC[C@H]1C(=O)NCC(=O)OCc1ccccc1

HCID13853221

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6422

未命名化合物

PROCEDURE

实验过程

2.0 g of Ac-Orn(Boc)-Pro-Gly-OBzl are dissolved in 5 ml of trifluoroacetic acid, and the solution is stirred at room temperature for 1 hour. After evaporation under high vacuum, 2.1 g of the trifluoroacetate of Ac-Orn-Pro-Gly-OBzl remain. Rf (system 2)=0.3; MS (FAB): 419 (M+1).

WORKUP

后处理

customAfter evaporation under high vacuum, 2.1 g of the trifluoroacetate of Ac-Orn-Pro-Gly-OBzl