HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86742670, compound → Oxiracetam
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86742670 | HCID 86742670 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Solvent | Water | HCID 962 | — |
| Product | Oxiracetam | HCID 4626 | — |
Reaction Steps
A solution of 0.65 g 2-methylpropyl 2-phenyl-4-oxoimidazolidine-β-hydroxybutanoate in 1.5 ml dimethyl sulfoxide and 0.5 ml water is heated at reflux for 16 h. After evaporating, the residue is chromatographed on silica, eluting with 7:3 ethyl acetate/methanol. Oxiracetam is obtained as a white powder, m.p. 167°-70° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04797496 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-070c1b7e2889487fa5f939515b7fc1bb |
| Source note | uspto-grants-1989_01 |