HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 13730721, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 86741235 | HCID 86741235 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 13730721 | HCID 13730721 | 63% |
Reaction Steps
A solution of N-(1-cyano-1,2-dimethylpropyl)maleamic acid (595 g, 2.83 mol) in acetic anhydride (3.96 liters) containing sodium acetate (13.72 g, 0.167 mol) is heated under reflux for one hour, cooled and the solvent removed in vacuo. The product is distilled* at 120°-130° C./0.1 mm to give 337 g (63%) of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04798619 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-3c97682a5ab14101b8d46ba7bbbf5ee1 |
| Source note | uspto-grants-1989_01 |