4-Nonanone → HCID 86742675, compound

HRID 2291813Notes

Reaction equation

HRID 2291813 reaction equation
[ClH:1].[NH2:2][OH:3].[CH3:4][CH2:5][CH2:6][C:7](=O)[CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]>C(O)C>[ClH:1].[CH3:4][CH2:5][CH2:6][C:7](=[N:2][OH:3])[CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 782364-NonanoneHCID 443297Hydroxyamine hydrochloride

Product 1

HCID 86742675HCID 86742675, compoundYield 75.3%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Hydroxylamine hydrochloride (2.1 g) was added to a solution of 1-azabicyclo[3.2.2.]nonan-4-one (2.77 g) in ethanol (30 ml) and the mixture was heated under reflux for 2 h. On cooling the reaction mixture to room temperature, the white solid was collected by filtration and dried in vacuo to give the title compound (2.84 g, 75%).

Workup

  1. temperatureunder reflux for 2 h
  2. filtrationthe white solid was collected by filtration
  3. customdried in vacuo

Sources & evidence

ORD record
ord-702917c8f1c34ee79ad438ff9d481fef
Source dataset
uspto-grants-1989_01
Patent number
US04798829

Reaction notes

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