Hydrochloric Acid → HCID 13519127, compound

HRID 2291864Notes

Reaction equation

HRID 2291864 reaction equation
[CH3:1][C:2]([CH3:22])([CH2:6][CH2:7][CH2:8][O:9][C:10]1[CH:15]=[CH:14][C:13]([C:16]2[N:17]=[C:18]([CH3:21])[S:19][CH:20]=2)=[CH:12][CH:11]=1)[C:3]([O-:5])=[O:4].[Na+].Cl>O>[CH3:1][C:2]([CH3:22])([CH2:6][CH2:7][CH2:8][O:9][C:10]1[CH:15]=[CH:14][C:13]([C:16]2[N:17]=[C:18]([CH3:21])[S:19][CH:20]=2)=[CH:12][CH:11]=1)[C:3]([OH:5])=[O:4]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 23675389HCID 23675389, compound

Product 1

HCID 13519127HCID 13519127, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

In 50 ml of water was dissolved 1.0 g of sodium 2,2-dimethyl-5-[p-(2-methyl-4-thiazolyl)phenoxy]pentanoate obtained in EXAMPLE 22. The solution was neutralized with 10% hydrochloric acid. The precipitated crystals were taken out by filtration and washed with water to give the desired product, 2,2-dimethyl-5-[p-(2-methyl-4-thiazolyl)phenoxy]pentanoic acid as white crystals.

Workup

  1. filtrationThe precipitated crystals were taken out by filtration
  2. washwashed with water

Sources & evidence

ORD record
ord-91171047245347be9b2314b0eec977c4
Source dataset
uspto-grants-1989_01
Patent number
US04798838

Reaction notes

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