HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium thiocyanate → HCID 178489846, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium thiocyanate | HCID 516872 | — |
| Reactant | HCID 85594591 | HCID 85594591 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178489846 | HCID 178489846 | — |
Reaction Steps
A solution of 3-(4-methoxyphenyl)-2-oxo-1-aminopropane, hydrochloride (3.0 g, 14 mmole) and potassium thiocyanate (1.36 g, 14 mmole) in acetic acid (60 ml) was heated under reflux for 15 minutes. The reaction was cooled, diluted with water and the product was filtered and recrystallized from ethyl alcohol and dried to give the product was a solid (1.6 g, 52%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04798843 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-d4ae76cd6a5b4abb88caa831fdba5675 |
| Source note | uspto-grants-1989_01 |