HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium thiocyanate → HCID 178490006, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium thiocyanate | HCID 516872 | — |
| Reactant | HCID 131715821 | HCID 131715821 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178490006 | HCID 178490006 | 19.2% |
Reaction Steps
A solution of 4-(4-methoxyphenyl)-2-oxo-1-aminobutane, hydrochloride (8.6 g, 37.7 mmole) and potassium thiocyanate (3.6 g, 37.7 mmole) in acetic acid (100 ml) was heated under reflux for 20 minutes. The reaction was cooled, diluted with water and the product was filtered and recrystallized from ethyl alcohol and dried to give the product as a solid (1.7 g, 19%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04798843 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-82cbcc68216644058c019003439d1711 |
| Source note | uspto-grants-1989_01 |