2,2,2-Trichloroethyl chloroformate → HCID 13936026, compound

HRID 2292038Notes

Reaction equation

HRID 2292038 reaction equation
Cl[C:2](Cl)(Cl)[CH2:3]OC(Cl)=O.[OH:10][CH:11]1[C:16](=[O:17])[NH:15][C:14]([CH3:18])=[CH:13][S:12]1>N1C=CC=CC=1>[OH:10][CH:11]1[C:16](=[O:17])[NH:15][C:14]([CH3:18])=[C:13]([C:3]2[CH:2]=[CH:16][N:15]=[CH:14][CH:13]=2)[S:12]1

Participants

4

Reactant 2

HCID 870632,2,2-Trichloroethyl chloroformateHCID 21277739HCID 21277739, compound

Product 1

HCID 13936026HCID 13936026, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

A mixture of pyridine, 2,2,2-trichloroethylchloroformate and 2-hydroxy-5-methyl-2H-1,4-thiazin-3(4H)-one was treated in the same manner as described in Example 6. The residue was recrystallized from ethanol to give the titled compound as pale yellow crystals.

Workup

  1. additionwas treated in the same manner
  2. customThe residue was recrystallized from ethanol

Sources & evidence

ORD record
ord-6b540a8a25874b919febac7cbf4703b6
Source dataset
uspto-grants-1989_01
Patent number
US04800201

Reaction notes

Loading…