HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2,2-Trichloroethyl chloroformate → HCID 13936026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2,2-Trichloroethyl chloroformate | HCID 87063 | — |
| Reactant | HCID 21277739 | HCID 21277739 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 13936026 | HCID 13936026 | — |
Reaction Steps
A mixture of pyridine, 2,2,2-trichloroethylchloroformate and 2-hydroxy-5-methyl-2H-1,4-thiazin-3(4H)-one was treated in the same manner as described in Example 6. The residue was recrystallized from ethanol to give the titled compound as pale yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04800201 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-6b540a8a25874b919febac7cbf4703b6 |
| Source note | uspto-grants-1989_01 |