4-Hydroxybenzophenone → HCID 14010384, compound

HRID 2292200Notes

Reaction equation

HRID 2292200 reaction equation
[OH:1][C:2]1[CH:15]=[CH:14][C:5]([C:6]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:7])=[CH:4][CH:3]=1.[CH:16]1([C:19](Cl)=[O:20])[CH2:18][CH2:17]1>N1C=CC=CC=1>[CH:16]1([C:19]([O:1][C:2]2[CH:3]=[CH:4][C:5]([C:6]([C:8]3[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=3)=[O:7])=[CH:14][CH:15]=2)=[O:20])[CH2:18][CH2:17]1

Participants

4

Reactant 2

HCID 143474-HydroxybenzophenoneHCID 77637Cyclopropanecarbonyl chloride

Product 1

HCID 14010384HCID 14010384, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Prepared from 6.0 g of 4-hydroxybenzophenone and 4.1 ml of cyclopropanecarbonyl chloride in 70 ml of pyridine. Recrystallized from ethyl acetate-ethanol-water mixture; M.P.~81°-81.5° C.

Workup

  1. customRecrystallized from ethyl acetate-ethanol-water mixture

Sources & evidence

ORD record
ord-246e51689a274516992a68318b80579e
Source dataset
uspto-grants-1989_01
Patent number
US04801610

Reaction notes

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