HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → 1-Ethoxy-3-fluorobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | 3-Fluorophenol | HCID 9743 | — |
| Product | 1-Ethoxy-3-fluorobenzene | HCID 136301 | — |
Reaction Steps
3-fluoro-phenol and ethyl iodide were reacted to form 3-fluoro-ethoxy benzene with a refractive index of nD25 =1.4823 which was reacted with nitric acid to obtain 2-ethoxy-4-fluoronitro benzene with a melting point of 28°~30° C. which was reacted to obtain 0-(4-nitro-3-ethoxy-phenyl)-hydroxylamine melting at 97°~98° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04801717 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-a3f6604296374e928ce3cd1f97c54e7b |
| Source note | uspto-grants-1989_01 |