HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 4'-Fluoro-3'-nitroacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 4'-Fluoroacetophenone | HCID 9828 | — |
| Product | 4'-Fluoro-3'-nitroacetophenone | HCID 2734612 | — |
Reaction Steps
1-fluoro-4-acetyl-benzene was reacted with nitric acid to obtain 2-fluoro-5-acetyl-nitro benzene with a melting point of 56°-58° C. which was reacted as in Example 1 to obtain 0-(4-acetyl-2-nitro-phenyl)-hydroxylamine melting at 132° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04801717 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-a16b1f1e22e545488e8422425ef21c43 |
| Source note | uspto-grants-1989_01 |