Ethyl Acetate → HCID 14390897, compound

HRID 2292332Notes

Reaction equation

HRID 2292332 reaction equation
[OH:1][C:2]1[CH:3]=[C:4]([CH:13]=[CH:14][C:15]=1[OH:16])[C:5]([N:7]1[CH2:11][CH2:10][NH:9][C:8]1=[O:12])=[O:6].CN([Si](C)(C)C)[C:19](=[O:24])[C:20](F)(F)F.[C:29](OCC)(=[O:31])[CH3:30]>>[C:19]([O:1][C:2]1[CH:3]=[C:4]([CH:13]=[CH:14][C:15]=1[O:16][C:29](=[O:31])[CH3:30])[C:5]([N:7]1[CH2:11][CH2:10][NH:9][C:8]1=[O:12])=[O:6])(=[O:24])[CH3:20]

Participants

4

Reactant 3

HCID 8857Ethyl AcetateHCID 32510N-methyl-N-(trimethylsilyl)trifluoroacetamideHCID 14390898HCID 14390898, compound

Product 1

HCID 14390897HCID 14390897, compound

Procedure

1-(3,4-Dihydroxybenzoyl)-2-imidazolidinone (2.2 g, 0.01 mol) was suspended in 70 ml of ethyl acetate. To the suspension was added 6.1 ml (0.033 mol) of N-methyl-N-(trimethylsilyl)trifluoroacetamide with stirring. After 30 minutes, a clear solution was formed (solution A).

Sources & evidence

ORD record
ord-cf57810c4b984f0aaafe8b35076f737c
Source dataset
uspto-grants-1989_01
Patent number
US04801705

Reaction notes

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