Hexanal → HCID 21477967, compound

HRID 2292408Notes

Reaction equation

HRID 2292408 reaction equation
C([Li])CCC.[CH:6](=[O:12])[CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].[F:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1[F:20]>>[F:13][C:14]1[C:15]([F:20])=[CH:16][CH:17]=[CH:18][C:19]=1[CH:6]([OH:12])[CH2:7][CH2:8][CH2:9][CH2:10][CH3:11]

Participants

4

Reactant 3

HCID 6184HexanalHCID 97061,2-DifluorobenzeneHCID 178418339Butyllithium

Product 1

HCID 21477967HCID 21477967, compound

Procedure

Quantities: n-butyllithium (31 cm3, 10.0M in hexanes, 0.31 mol), hexanal (31.5 g, 0.31 mol) and 1,2-difluorobenzene (35.5 g, 0.31 mol). The experimental procedure was as described in Example 16.

Sources & evidence

ORD record
ord-d760541cdc784819a694d99f2c6f7c5f
Source dataset
uspto-grants-1997_11
Patent number
US05683623

Reaction notes

Loading…