HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxide (P4O10) → 2,3-Difluoro-1-octylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxide (P4O10) | HCID 14812 | — |
| Reactant | 1-(2,3-Difluorophenyl)octan-1-ol | HCID 53699850 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 2,3-Difluoro-1-octylbenzene | HCID 14495629 | — |
Reaction Steps
Quantities: compound from Example 19 (53.3 g, 0.22 mol), phosphorus pentoxide (95 g, 0.67 mol) and 5% palladium-on-charcoal (5.5 g). The experimental procedure was as described in Example 22.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05683623 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-c569c470e2054be3a43919ece44e7e33 |
| Source note | uspto-grants-1997_11 |