HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxide (P4O10) → 1-Decyl-2,3-difluorobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxide (P4O10) | HCID 14812 | — |
| Reactant | (2,3-Difluorophenyl)decan-1-ol | HCID 21477954 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 1-Decyl-2,3-difluorobenzene | HCID 21477945 | — |
Reaction Steps
Quantities: compound from Example 21 (56.4 g, 0.21 mol), phosphorus pentoxide (74.5 g, 0.53 mol) and 5% palladium-on-charcoal (4.58). The experimental procedure was as described in Example 22.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05683623 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-500d918177684402bdf015e9f0b33816 |
| Source note | uspto-grants-1997_11 |