HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 53883511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 54184109 | HCID 54184109 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 53883511 | HCID 53883511 | — |
Reaction Steps
By the method of Example 1, Step E, 18.27 grams (0.073 mole) of 2,3-dichloro-5-nitrophenylacetic acid and 80 mL of thionyl chloride were reacted in 400 mL of carbon tetrachloride, yielding 20.90 grams of 2,3-dichloro-5-nitrophenylacetyl chloride. The NMR was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05683966 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-8afd02ddc08d4631a84bdb464260499d |
| Source note | uspto-grants-1997_11 |