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HRID2292471

反应详情

EQUATION

反应方程式

HRID 2292471 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)c1cc(S)cc(C(C)(C)C)c1O
HCID70370

2,6-Di-tert-butyl-4-mercaptophenol

C14H22OS

结构：CCOC(=O)/N=N/C(=O)OCC
HCID5462977

(E)-Diethyl azodicarboxylate

C6H10N2O4

PRODUCTS

生成物

2
结构：CC(C)(C)c1cc(S)cc(C(C)(C)C)c1O
HCID70370

2,6-Di-tert-butyl-4-mercaptophenol

C14H22OS

结构：CCOC(=O)N=NC(=O)OCC
HCID220568

Diethyl azodicarboxylate

C6H10N2O4

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

Combine 3,5-di-t-butyl-4-hydroxythiophenol (751 mg), diethylazodicarboxylate (496μL, 3.15 mmol) and p-dioxane (5 mL). Place under an argon atmosphere and stir for 2 hours to give a complex of 3,5-di-t-butyl-4-hydroxythiophenol and diethyl azodicarboxylate.