HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 131720266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | HCID 21478661 | HCID 21478661 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131720266 | HCID 131720266 | 34.7% |
Reaction Steps
To a solution containing 0.26 g of the compound of Example 214 in methanol, 59 mg of fumaric acid in methanol is added and the resulting mixture is condensed. To the resultant, isopropanol and isopropyl ether are added. The resultant is subjected to filtration and the filtrate is dried to obtain 0.11 g of (214) in the form of amorphous.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05683998 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-800e99d3ac034986b19f31a8fa8a364c |
| Source note | uspto-grants-1997_11 |