HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylsulphonyl isocyanate → HCID 53939961, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylsulphonyl isocyanate | HCID 76096 | — |
| Reactant | HCID 12752076 | HCID 12752076 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 53939961 | HCID 53939961 | — |
Reaction Steps
Combine 2-(4-methoxybenzoyl)-chromone (1 mmol) and benzenesulfonyl isocyanate (1.2 mmol) in acetonitrile (7.0 mL). Heat at reflux for 48 hours. Add methanol (5 mL) to quench the reaction. Evaporate in vacuo. Recrystallize to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05684017 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-262fee82fdf24d48ba1ef2d75e0c73cc |
| Source note | uspto-grants-1997_11 |