HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxybenzyl chloride → HCID 21479361, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxybenzyl chloride | HCID 69994 | — |
| Reactant | 1-(Bromomethyl)-4-(trifluoromethoxy)benzene | HCID 142785 | — |
| Reactant | HCID 178524040 | HCID 178524040 | — |
| Product | HCID 21479361 | HCID 21479361 | — |
Reaction Steps
Following the procedure of Example 26(c)-26(d), except substituting ethyl 1-(2-chloro-4,5-methylenedioxybenzyl)-5-hydroxy-3-phenylindole-2-carboxylate for 1-(2-chloro-4,5-methylenedioxybenzyl)-3-(3,5-dichlorophenyl)-5-hydroxyindole-2-carboxylate and 3-methoxybenzyl chloride for 4-trifluoromethoxybenzyl bromide in step (c), the title compound was prepared as a white solid (64% overall). MS (MH+): 542.4
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05684032 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-701ffeebb6744bbcb22ed17495d9a701 |
| Source note | uspto-grants-1997_11 |