Sodium Azide → HCID 178437402, compound

HRID 2292740Notes

Reaction equation

HRID 2292740 reaction equation
[CH2:1]([C:3]1[N:7]([CH2:8][C:9]2[CH:14]=[CH:13][C:12]([C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=3[C:21]#[N:22])=[CH:11][CH:10]=2)[C:6]2[CH:23]=[C:24]([C:27]3[N:31]([CH3:32])[C:30]4[CH:33]=[CH:34][CH:35]=[CH:36][C:29]=4[N:28]=3)[CH:25]=[CH:26][C:5]=2[N:4]=1)[CH3:2].[N-:37]=[N+:38]=[N-:39].[Na+]>CN(C)C=O>[CH2:1]([C:3]1[N:7]([CH2:8][C:9]2[CH:10]=[CH:11][C:12]([C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=3[C:21]3[NH:39][N:38]=[N:37][N:22]=3)=[CH:13][CH:14]=2)[C:6]2[CH:23]=[C:24]([C:27]3[N:31]([CH3:32])[C:30]4[CH:33]=[CH:34][CH:35]=[CH:36][C:29]=4[N:28]=3)[CH:25]=[CH:26][C:5]=2[N:4]=1)[CH3:2]

Participants

4

Reactant 2

HCID 33557Sodium AzideHCID 21479190HCID 21479190, compound

Product 1

HCID 178437402HCID 178437402, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Prepared analogously to Example 41 from 4'-[[2-ethyl-6-(1-methyl-benzimidazol-2-yl)-benzimidazol-1-yl]methyl]-2-cyano-biphenyl and sodium azide in dimethylformamide.

Sources & evidence

ORD record
ord-6502b7e5de624805bcf4094b1b4fcf39
Source dataset
uspto-grants-1997_11
Patent number
US05684029

Reaction notes

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