HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 21475502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 21475500 | HCID 21475500 | — |
| Reactant | 2-Nitro-N~1~-(prop-2-en-1-yl)benzene-1,4-diamine | HCID 23500036 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21475502 | HCID 21475502 | — |
Reaction Steps
A mixture consisting of N-(2-nitro-4-aminophenyl)-allylamine (1.9 g, 0.01 mole), allyl bromide (2.4 g, 0.02 mole) and potassium carbonate (2.8 g, 0.02 mole) was boiled under reflux for 7 hours in 20 ml of ethanol. Working up was carried out in the same way as for compound 4. Yellow crystals, melting point 131°-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05685881 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-dd728f2852074dec8a9aa9ea94d068ee |
| Source note | uspto-grants-1997_11 |