Phenethylamine → HCID 3798338, compound

HRID 2293130Notes

Reaction equation

[CH2:1]([NH2:9])[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:10](Cl)(=O)[CH2:11][CH3:12]>>[CH2:11]([CH:12]1[C:8]2[C:3](=[CH:4][CH:5]=[CH:6][CH:7]=2)[CH2:2][CH2:1][NH:9]1)[CH3:10]

Participants

Reactant 2

HCID 1001Phenethylamine

HCID 62324Propionyl chloride

Product 1

HCID 3798338HCID 3798338, compound

Procedure

In accordance with the same procedures as in Preparation 1-1, except that 11.3 ml of phenethylamine (90 mM) and 7.8 ml of propionyl chloride(90 mM) were used as starting materials, 8.48 g of the title compound was prepared.

Workup

customIn accordance with the same procedures as in Preparation 1-1

Sources & evidence

ORD record: ord-8012cdda06f54b45b32bca5a0874a1fb
Source dataset: uspto-grants-1997_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05686458

Reaction notes

Loading…