HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 21476517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | Glycine, N-[1-(2-methylphenyl)ethyl]-, ethyl ester | HCID 21476429 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21476517 | HCID 21476517 | 73.1% |
Reaction Steps
To a mixture of 3.8 g of lithium aluminium hydride (0.1M) and 150 ml of tetrahydrofuran, 23.3 g of the compound (0.105M) prepared in Step 2 above was dropwise added at room temperature and stirred for 30 minutes. The resultant was added with water and solids produced were filtered. The filtrate was dried over anhydrous sodium sulfate and concentrated under a reduced pressure, to give 13.8 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686458 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-d27c09a32e4e4329baf030e0a5a47bc3 |
| Source note | uspto-grants-1997_11 |