2-Methoxyethylamine → HCID 86613128, compound

HRID 229342Notes

Reaction equation

HRID 229342 reaction equation
[C:1](#[N:10])[CH:2]=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[CH3:11][C:12]1[NH:16][N:15]=[C:14]([NH2:17])[CH:13]=1.[CH3:18][O:19][CH2:20][CH2:21][NH2:22]>>[CH3:18][O:19][CH2:20][CH2:21][NH:22][C:3]1[CH:2]=[C:1]([NH:17][C:14]2[CH:13]=[C:12]([CH3:11])[NH:16][N:15]=2)[N:10]=[C:1]([CH:2]=[CH:3][C:4]2[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=2)[N:10]=1

Participants

4

Reactant 3

HCID 80182-MethoxyethylamineHCID 746673-Phenylprop-2-enenitrileHCID 931461H-Pyrazol-3-amine, 5-methyl-

Product 1

HCID 86613128HCID 86613128, compound

Procedure

Example 163 was synthesized via Scheme 6 according to the general scheme provided above with the appropriate starting materials cinnamonitrile, 5-methyl-1H-pyrazole-3-amine, and 2-methoxyethanamine. Structure of the target was confirmed by 1H-NMR. The 1H-NMR is attached.

Workup

  1. customExample 163 was synthesized via Scheme 6 according to the general scheme
  2. customprovided above with the

Sources & evidence

ORD record
ord-4c648f9e8a684f6a84a7fbbc5716a06b
Source dataset
uspto-grants-2009_07
Patent number
US07563787B2

Reaction notes

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