HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131720304, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Tetrafluoro-m-phenylenediamine dihydrochloride | HCID 149026 | — |
| Reactant | HCID 131720305 | HCID 131720305 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 131720304 | HCID 131720304 | — |
Reaction Steps
Following the procedure described in Example 120, the coupling of N-[2-(3,4,5-trimethoxyphenyl)-2-oxoethyl] -L-proline hydrochloride (300 mg, 0.83 mmol) and 2(2-aminoethyl)pyridine (0.4 mL, 2.5 mmol ) provided, after treatment with HCl in Et2O, 193 mg of the dihydrochloride salt of L-proline, 1-[2-(3,4,5-trimethoxyphenyl)-2-oxoethyl] 2-(pyrid-2-yl)ethylamide as a powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686424 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-3e774cdc229c4aa8b08edc0c4f7852c4 |
| Source note | uspto-grants-1997_11 |