HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67619574, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67619575 | HCID 67619575 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67619574 | HCID 67619574 | — |
Reaction Steps
Following the procedure described in Example 120, the coupling of N-[2-(3,4,5-trimethoxyphenyl)-2-oxoethyl] -L-proline hydrochloride (250 mg, 0.69 mmol) and cyclohexylamine (0.24 mL, 2.1 mmol) provided, after treatment with HCl in Et2O, 147 mg of the hydrochloride salt of L-proline, 1-[2-(3,4,5-trimethoxyphenyl)-2-oxoethyl] cyclohexylamide as a powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686424 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-06a4a475ca3644deb670cff26b1f1870 |
| Source note | uspto-grants-1997_11 |