HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propylvaleryl chloride → HCID 22879053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propylvaleryl chloride | HCID 76240 | — |
| Reactant | HCID 22873003 | HCID 22873003 | — |
| Product | HCID 22879053 | HCID 22879053 | 60% |
Reaction Steps
Using the procedure described in Example 7, treatment of 1-[2-(S)-amino-4-methylpentyl]-L-proline 4-phenylbutylamide (20 mg) with di-n-propylacetyl chloride(14 uL) provided 16 mg (60%) of the title compound. The 1H NMR and Mass spectrum analysis of this compound was consistent with the structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686469 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-60e2d3c6c8804f27825e6ed0ad28ec78 |
| Source note | uspto-grants-1997_11 |