HuagongsheHuagongshe Chemistry Print Report · For research reference only
9-Fluorenone-4-carbonyl chloride → HCID 22879061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 9-Fluorenone-4-carbonyl chloride | HCID 610142 | — |
| Reactant | HCID 22873003 | HCID 22873003 | — |
| Product | HCID 22879061 | HCID 22879061 | 18% |
Reaction Steps
Using the procedure described in Example 7, treatment of 1-[2-(S)-amino-4-methylpentyl ]-L-proline 4-phenylbutylamide (134 mg) with 9-fluorenone-4-carbonyl chloride (131 mg) provided 35 mg(18%) of the title compound. The 1H NMR and Mass spectrum analysis of this compound was consistent with the structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686469 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-35c894c60b4842a78375af59806588d1 |
| Source note | uspto-grants-1997_11 |