huagongshe.com
HRID2293595

反应详情

EQUATION

反应方程式

HRID 2293595 的结构方程式

REACTANTS

反应物

1
结构：CCCCC(F)(F)C(=O)C=C[C@@H]1[C@H]2CC(=O)O[C@H]2C[C@H]1OC1CCCCO1
HCID57165886

未命名化合物

PRODUCTS

生成物

1
结构：CCCCC(F)(F)C(=O)CC[C@@H]1[C@H]2CC(=O)O[C@H]2C[C@H]1OC1CCCCO1
HCID15222216

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

The compound (50) (12.7 g) was catalytically hydrogenated over 5% palladium on carbon (catalytic amount) in ethyl acetate (300 ml) under hydrogen atmosphere to give the titled compound (51). Yield: 12.5 g (99%).