Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | HCID 21477483 | HCID 21477483 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 10631480 | HCID 10631480 | — |
Reaction Steps
NaCN (509 mg) in DMSO (4.25 ml) is added to 4-(6-chlorohexyl)pyridine (1.71 g) dissolved in DMSO (4.25 ml). The mixture is stirred at 60° C. for 3 hours, poured into water (100 ml) and extracted with chloroform (3×15 ml). The combined extracts are washed with water (2×20 ml), dried (Na2SO4) and the solvent evaporated to give 4-(6-cyanohexyl)-pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05686564 |
|---|
| Source dataset | uspto-grants-1997_11 |
|---|
| ORD ID | ord-8788f0f681684b998d3dd3813bef10b4 |
|---|
| Source note | uspto-grants-1997_11 |
|---|
