HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxybenzaldehyde → HCID 54737842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxybenzaldehyde | HCID 101 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | 4-Hydroxycoumarin | HCID 54682930 | — |
| Reactant | HCID 178418443 | HCID 178418443 | — |
| Product | HCID 54737842 | HCID 54737842 | — |
Reaction Steps
Addition of ethylmagnesium bromide to 3-hydroxy benzaldehyde gives the compound of formula G-2, which can be alkylated with allyl bromide to give the compound of formula G-3. Reaction between 4-hydroxycoumarin and the compound of formula G-3 using boron trifluoride etherate as an acidic catalyst gives the compound of formula G-4 (for example, 3-(1'-(3-Allyloxyphenyl)propyl)-4-hydroxycoumarin.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686486 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-b0438fdc88ae4fa58dd6cf47d96c0331 |
| Source note | uspto-grants-1997_11 |