Ammonia → HCID 57757887, compound

Participants

Reaction Steps

To a suspension of diester 2 (10.9 g, 31.9 mmol) in 50 mL ethanol was added 50 mL of 7M methanolic ammonia at 23° C. After 3 h, the copious precipitate was collected by vacuum filtration and dried under a stream of air to give 7.45 g (74%) of amide 3 as a white solid.

Provenance & Evidence