Sodium Iodide → HCID 54724936, compound

Participants

Reaction Steps

To 96 mg (2 mmol) of the title compound of Example 331 is added 34 mg of NaI and 2 ml of methylene chloride. The reaction mixture is heated at reflux for 18 hours. The solution is cooled to room temperature and evaporated to dryness under vacuum. The residue is distributed between water and methylene chloride, the organic solution is washed twice with water, dried over anhydrous sodium sulfate, filtered and evaporated to dryness to give the title compound as an amorphous solid.

Provenance & Evidence