HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichloro-4-propyl-3-pyridinamine → HCID 21477769, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichloro-4-propyl-3-pyridinamine | HCID 21477768 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21477769 | HCID 21477769 | — |
Reaction Steps
In a 1 liter stirred autoclave 150.0 g of 3-amino-2,6-dichloro-4-n-propylpyridine and 5.0 g of 10% palladium/carbon are suspended in a mixture of 450.0 ml of methanol and 150.0 ml of water and hydrogenated under 3 bars of hydrogen at 50°-70° C. until the uptake of gas has ceased.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686618 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-8f3a544454be4c91a0f45f4f3f48b7d7 |
| Source note | uspto-grants-1997_11 |