HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21474274, compound → HCID 21474317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21474274 | HCID 21474274 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | HCID 21474317 | HCID 21474317 | — |
Reaction Steps
3-Benzyloxy-1-(2,3-dihydroxy-propyl)-2-(hydroxy-phenyl-methyl)-1H-pyridin-4-one: From 2.1 g of 3-benzyloxy-1-(2,3-dihydroxy-propyl)-2-[phenyl-(tetrahydropyran-2-yloxy)methyl]-1H-pyridin-4-one there is obtained analogously to Example 6e, after chromatography: 3-benzyloxy-1-(2,3-dihydroxy-propyl)-2-(hydroxy-phenyl-methyl)-1H-pyridin-4-one. Colourless foam, diastereoisomeric mixture. Rf value 0.22 (silica gel 60, dichloromethane/ethanol 4/1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05688815 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-cbd8224ab0cc482897a18aff37ce60cf |
| Source note | uspto-grants-1997_11 |