HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21474287, compound → HCID 21474470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21474287 | HCID 21474287 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | HCID 21474470 | HCID 21474470 | — |
Reaction Steps
3-Benzyloxy-1-(2-dimethylamino-ethyl)-2-(hydroxy-phenyl-methyl)-1H-pyridin-4-one: From 5.2 g of 3-benzyloxy-1-(2-dimethylamino-ethyl)-2-[phenyl-(tetrahydropyran-2-yloxy)-methyl]-1H-pyridin-4-one there is obtained analogously to Example 6e, after chromatography: 3-benzyloxy-1-(2-dimethylamino-ethyl)-2-(hydroxy-phenyl-methyl)-1H-pyridin-4-one. Beige, amorphous foam. Rf value: 0.16 (silica gel 60, dichloromethane/ethanol 4/1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05688815 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-90061a984c6c408eacd01d85e85c393d |
| Source note | uspto-grants-1997_11 |