HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21474425, compound → HCID 21474442, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21474425 | HCID 21474425 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | HCID 21474442 | HCID 21474442 | — |
Reaction Steps
3-Benzyloxy-2-(hydrox-pyridin-2-yl-methyl-1-methyl-1H-pyridin-4-one: From 2.5 g of 3-benzyloxy-1-methyl-2-[pyridin-2-yl-(tetrahydropyran-2-yloxy)-methyl]-1H-pyridin-4-one there is obtained analogously to Example 7b: 3-benzyloxy-2-(hydroxy-pyridin-2-yl-methyl)-1-methyl-1H-pyridin-4-one. Yellow resin. Rf value: 0.52 (silica gel 60, dichloromethane/ethanol 4/1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05688815 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-cc58c5eb8f4c42c1865db2327d82067a |
| Source note | uspto-grants-1997_11 |