Aluminium lithium hydride → HCID 21474807, compound

Participants

Reaction Steps

A procedure similar to that described in Preparation 13 was repeated, except that 6.22 g of 3-(3-chlorobenzyloxy)-2-hydroxypropylazide (prepared as described in Preparation 92), 1.97 g of lithium aluminum hydride and 120 ml of anhydrous tetrahydrofuran were used, to give 3.37 g of the title compound having an Rf value of 0.03 (on silica gel thin layer chromatography, using a mixture of ethyl acetate as the developing solvent).

Provenance & Evidence