HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,6,7,8-Tetrahydro-5,5,8,8-tetramethyl-2-naphthylmethanol → Allyl 4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylmethyloxycarbonyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,6,7,8-Tetrahydro-5,5,8,8-tetramethyl-2-naphthylmethanol | HCID 14425621 | — |
| Reactant | 4-(Allyloxycarbonyl)benzoic acid | HCID 18349855 | — |
| Product | Allyl 4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylmethyloxycarbonyl)benzoate | HCID 21474529 | — |
Reaction Steps
In a manner similar to Example 4(c), by reaction of 2.06 g (10 mmol) of 4-(allyloxycarbonyl)benzoic acid with 2.18 g (10 mmol) of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylmethanol, 2.8 g (70%) of allyl ester are obtained in the form of a translucent oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05688817 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-cb685f53cfee4d05a2a35381f87c10d6 |
| Source note | uspto-grants-1997_11 |