HuagongsheHuagongshe Chemistry Print Report · For research reference only
Prop-2-en-1-yl 4-aminobenzoate → Allyl 4-(alpha-fluoro-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylacetamido)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Prop-2-en-1-yl 4-aminobenzoate | HCID 13075143 | — |
| Reactant | alpha-Fluoro-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylacetic acid | HCID 21474586 | — |
| Product | Allyl 4-(alpha-fluoro-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylacetamido)benzoate | HCID 53834800 | — |
Reaction Steps
In a manner similar to Example 4(c), by reaction of 1.35 g (5.1 mmol) of α-fluoro-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylacetic acid with 920 mg (5.1 mmol) of allyl 4-aminobenzoate, 1.7 g (81%) of ester are obtained in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05688817 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-6876a97bed634594890e6c9eb6dd666c |
| Source note | uspto-grants-1997_11 |