HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanol → Cyclohexyl 5-amino-4-oxopentanoate--hydrogen chloride (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanol | HCID 7966 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Aminolevulinic Acid Hydrochloride | HCID 123608 | — |
| Product | Cyclohexyl 5-amino-4-oxopentanoate--hydrogen chloride (1/1) | HCID 22253131 | — |
Reaction Steps
From cyclohexanol (6.0 ml) and 5-amino-4-oxopentanoic acid hydrochloride (1.0 g; 6.0 mmol) at 80° C. Thionyl chloride was added at room temperature. The reaction was complete after 3 h. The yield was 1.48 g (99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07563819B1 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-3b16eaa2e69f4a5cab47b1ead0702698 |
| Source note | uspto-grants-2009_07 |