HCID 21471076, compound → HCID 21471077, compound

Participants

Reaction Steps

3.17 g (0.01M) of 2-(m-chlorobenzamido)-2-(p-tolyl)propionic acid was dissolved in 30 ml of acetic anhydride and the resulting solution was heated for 1 hr with reflux. The reaction solution was cooled and distilled out acetic anhydride in vacuo. The residue was subjected to chromatography, to give 2.4 g of the object compound, pure oily compound: 80 % Yield.

Provenance & Evidence