HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzenesulfonyl isocyanate → HCID 10811871, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzenesulfonyl isocyanate | HCID 138587 | — |
| Reactant | Glycine, N-(4-chlorophenyl)-, methyl ester | HCID 11298576 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 10811871 | HCID 10811871 | 97.5% |
Reaction Steps
Three grams (15 mmol) of methyl 4-chlorophenylaminoacetate were dissolved in 40 ml of benzene, and 2.2 ml (15 mmol) of 4-chlorobenzenesulfonyl isocyanate were added to the resultant solution, followed by stirring for 1 hour. Crystals formed were collected by filtration to obtain N-(4-chlorobenzenesulfonyl)-N'-(4-chlorophenyl)-N'-methoxycarbonylmethylurea (6.1 g) as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05691335 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-7d9b3ce45bba4a698289daa6aee57ff6 |
| Source note | uspto-grants-1997_11 |