HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluorobenzylic alcohol → HCID 17989813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluorobenzylic alcohol | HCID 67969 | — |
| Reactant | Aminolevulinic Acid Hydrochloride | HCID 123608 | — |
| Product | HCID 17989813 | HCID 17989813 | — |
Reaction Steps
From 2-fluorobenzyl alcohol (5.7 g; 45 mmol) and 5-amino-4-oxopentanoic acid hydrochloride (1.0 g; 6.0 mmol). The reaction was complete after 27 h at 100° C. The yield was 0.64 g (44%). Mp 91-94° C. (dec.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07563819B1 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-1ff243290f144ce7a854d10249014356 |
| Source note | uspto-grants-2009_07 |