HCID 22100389, compound → HCID 21472345, compound

Participants

Reaction Steps

1.04 g (3.66 mmole) of the compound obtained in step 6 was dissolved in 5 ml of CH2Cl2 and thereto was added 3.2 g (36.6 mmole) of activated MnO2. The reaction solution was stirred for 16 hours at room temperature and filtered through Cellite. The resultant was concentrated under reduced pressure to obtain 0.57 g of the title compound (yield 55%).

Provenance & Evidence