HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-methylbutane → HCID 21472394, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-methylbutane | HCID 7891 | — |
| Reactant | 4-Iodophenol | HCID 10894 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(ALLYLOXY)BENZONITRILE | HCID 257949 | — |
| Product | HCID 21472394 | HCID 21472394 | — |
Reaction Steps
Using the method described in Example 48 for the preparation of 4-cyanophenol allyl ether, 4-iodophenol was reacted with isoamylbromide in the presence of potassium carbonate to give 4-iodo-isoamyloxyphenol as an oil, NMR(CDCl3): 0.95(6H,d), 1.66(2H,q), 1.68-1.92(1H,m), 3.93(2H,t), 6.63-6.72(2H,d), 7.49-7.59(2H,d); m/z290(M).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05691349 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-9c394f6504b0487dbbe520f3b465ab12 |
| Source note | uspto-grants-1997_11 |