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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2294966Generated: October 31, 2026

1-Bromo-3-methylbutane → HCID 21472394, compound

https://huagongshe.com/reaction/2294966

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Bromo-3-methylbutaneHCID 7891—
Reactant4-IodophenolHCID 10894—
ReactantPotassium CarbonateHCID 11430—
Reactant4-(ALLYLOXY)BENZONITRILEHCID 257949—
ProductHCID 21472394HCID 21472394—

Reaction Steps

Using the method described in Example 48 for the preparation of 4-cyanophenol allyl ether, 4-iodophenol was reacted with isoamylbromide in the presence of potassium carbonate to give 4-iodo-isoamyloxyphenol as an oil, NMR(CDCl3): 0.95(6H,d), 1.66(2H,q), 1.68-1.92(1H,m), 3.93(2H,t), 6.63-6.72(2H,d), 7.49-7.59(2H,d); m/z290(M).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05691349
Source datasetuspto-grants-1997_11
ORD IDord-9c394f6504b0487dbbe520f3b465ab12
Source noteuspto-grants-1997_11